Course Information


Course Information
Course Title Code Semester L+U Hour Credits ECTS
INSTRUMENTAL ANALYSIS KİM429 7. Semester 3 + 2 4.0 7.0

Prerequisites None

Language of Instruction Turkish
Course Level Bachelor's Degree
Course Type Compulsory
Mode of delivery
Course Coordinator
Instructors Orhan ATAKOL
Assistants
Goals To transfer the benefits of instrumental analysis methods in analytical chemistry . Transfer of the analysis time, systematic errors and the limits of determination to the desired changes by instrumental analysis methods. Presentation of basic spectroscopic methods. Infra-ultraviolet-visible field, Infrared, NMR, AAS and MS methods are shown in detail and students can interpret the spectral output of these methods.
Course Content Classification of instrumental analysis methods, Introduction to spectroscopy. Principles of spectroscopic methods. Atomic spectroscopy, AAS and AES. Molecular spectroscopy, Ultraviolet - Visible field spectroscopy, Luminescence, IR spectroscopy, NMR methods. Spectrum solution for structure analysis.
Learning Outcomes 1) Classify instrumental analysis methods and compare them with each other.
2) recognize the different units of various devices and explains their properties.
3) Interprets the schematic of the instrument and its working principle.
4) Compares the limits of determination of instrumental analysis methods with those of classical methods.

Weekly Topics (Content)
Week Topics Teaching and Learning Methods and Techniques Study Materials
1. Week Light and its properties, characterizing parameters Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
2. Week Electromagnetic spectrum and effects on the matter Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
3. Week Introduction to atomic spectroscopy Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
4. Week Atomic Absorption methods, background corrections, devices. Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
5. Week LOD, LOQ and kalibration in AAS methods. Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
6. Week AES methods, ICP devices. Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
7. Week Introduction to molecular spectroscopy, principles. Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
8. Week Lambert-Beer Law and UV-VIS devices. Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
9. Week Luminescence methods, florimeters. Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
10. Week Introduction to IR spectroscopy, principles and applications. Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
11. Week IR , FTIR devices. Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
12. Week Nuclear magnetic resonance, basics and Principles Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
13. Week Spin-spin splitting, first order spectra. Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
14. Week 13C NMR method Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
15. Week Structure solution using IR and NMR data Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework
16. Week Mass spectrometry, ionisation and dedection methods. EI,CI,FI,ESI,MALDI Lecture; Question Answer; Problem Solving
Brainstorming
Problem Based Learning 		Homework

Sources Used in This Course
Recommended Sources
B.C. Smith, Fundamentals of Fourier Infrared Spectroscopy, CRC Press, Second Edition, 2011.
D.A. Skoog, F.J. Holler, S.R. Crouch, Principles of Instrumental Analysis, Sixth Edition, Thomson Brooks/cole, 2007. D.A. Skoog, F.J. Holler, S.R. Crouch, Principles of Instrumental Analysis, Sixth Edition, Thomson Brooks/cole, 2007.
D.A. Skoog, F.J. Holler, T.A. Nieman, Instrumental Analiz İlkeleri, Çeviri Editörleri E.Kılıç, H.Yılmaz, F. Köseoğlu, Bilim Yayıncılık 1999. D.A. Skoog, F.J. Holler, T.A. Nieman, Instrumental Analiz İlkeleri, Çeviri Editörleri E.Kılıç, H.Yılmaz, F. Köseoğlu, Bilim Yayıncılık 1999.
D.A. Skoog, J.J. Leary, Instrumental Analitik, Springer, 1996.
R.Flamini, P.Traldi, Mass Spectrometry in Grape and Wine Chemistry, J.Wiley & Sons, 2010.
R.M. Silverstein, F.X. Webster, D.J. Kiemle, Spectrometric Idenfication of Organic Compounds, J.Wiley &Sons, Seventh edition, 2005.

Relations with Education Attainment Program Course Competencies
Program RequirementsContribution LevelDK1DK2DK3DK4
PY150050
PY250000
PY350000
PY450050
PY550000

*DK = Course's Contrubution.
0 1 2 3 4 5
Level of contribution None Very Low Low Fair High Very High
.

ECTS credits and course workload
Event Quantity Duration (Hour) Total Workload (Hour)
Course Duration (Total weeks*Hours per week) 14 5
Work Hour outside Classroom (Preparation, strengthening) 14 5
Homework 2 10
Midterm Exam 2 2
Time to prepare for Midterm Exam 2 10
Final Exam 1 2
Time to prepare for Final Exam 1 10
Total Workload
Total Workload / 30 (s)
ECTS Credit of the Course
Quick Access Hızlı Erişim Genişlet
Course Information
  • Course Information
  • Weekly Topics (Content)
  • Sources Used in This Course
  • Relations with Education Attainment Program Course Competencies
  • ECTS credits and course workload