Course Information


Course Information
Course Title Code Semester L+U Hour Credits ECTS
SPECTROSCOPIC METHODS IN ORGANIC CHEMISTRY II 801300715680 3 + 0 3.0 8.0

Prerequisites None

Language of Instruction Turkish
Course Level Graduate Degree
Course Type Compulsory
Mode of delivery face to face
Course Coordinator
Instructors
Assistants
Goals To introduce the basic concepts of 13C-NMR, 2D-NMR and mass spectroscopies and identification the structure and composition of an unknown organic compound by combined application of spectroscopic methods.
Course Content Basic concepts of 13C-NMR spectroscopy, two-dimensional NMR spectroscopy, (COSY, HETCOR, INADEQUATE, NOESY techniques), mass spectroscopy, (EI, CI, FI, FD, FAB, SIMS techniques) and structural analyses of organic compounds using 13C-NMR and mass spectroscopies.
Learning Outcomes 1) 1.The student defines the priciples of spectroscopy in organic chemistry.
2) 2. The student will be able to interpret 1H-NMR ve 13C-NMR spectroscopies and to analyse the chemical structure.
3) 3.The student will be able to interpret MS and to analyse the chemical structure.
4) 4. The student will be able to identify the structure and composition of an unknown organic compound by combined application of UV-VIS, IR, NMR methods.
5) 5. The student will be able to identify the structure and composition of an unknown organic compound by combined application of UV-VIS, IR, NMR and MS methods.

Weekly Topics (Content)
Week Topics Teaching and Learning Methods and Techniques Study Materials
1. Week Fundamental principal of spectroscopy Lecture

 Presentation (Including Preparation Time)
2. Week 13C-NMR spectroscopy: Fundamental principles Lecture

 Presentation (Including Preparation Time)
3. Week Interpretation of 1H-NMR and 13C-NMR spectra and structural analysis Lecture

 Presentation (Including Preparation Time)
4. Week Spin-spin coupling Lecture

 Presentation (Including Preparation Time)
5. Week Interpretation of coupled and decoupled spectra and structural analysis Lecture

 Presentation (Including Preparation Time)
6. Week 2D-NMR techniques Lecture

 Presentation (Including Preparation Time)
7. Week Interpretation of COSY, HETCOR, NOESY spectra and structural analysis Lecture

 Presentation (Including Preparation Time)
8. Week Interpretation of IR, COSY, HETCOR, NOESY spectra and structural analysis Lecture

 Presentation (Including Preparation Time)
9. Week Mass Spectrscopy: Fundamental principals Lecture

 Presentation (Including Preparation Time)
10. Week Formation of fragmans of ions Lecture

 Presentation (Including Preparation Time)
11. Week Interpretation of mass spectra and structural analysis Lecture

 Presentation (Including Preparation Time)
12. Week Interpretation of 1H-NMR, 13C-NMR and mass spectra and structural analysis Lecture

 Presentation (Including Preparation Time)
13. Week Interpretation of 1H-NMR, 13C-NMR and mass spectra and structural analysis Lecture

 Presentation (Including Preparation Time)
14. Week Interpretation of IR, NMR and mass spectra and structural analysis Lecture

 Presentation (Including Preparation Time)

Sources Used in This Course
Recommended Sources
1. Spectrometric Identification of Organic Compounds, Silverstein
2. Introduction to Spectroscopy, Pavia
3. İlgili bilimsel makaleler

ECTS credits and course workload
Event Quantity Duration (Hour) Total Workload (Hour)
Course Duration (Total weeks*Hours per week) 14 3
Work Hour outside Classroom (Preparation, strengthening) 14 3
Homework 9 1
Report (Including Preparation and presentation Time) 9 1
Activity (Web Search, Library Work, Trip, Observation, Interview etc.) 14 1
Midterm Exam 3 2
Time to prepare for Midterm Exam 3 2
Final Exam 1 3
Time to prepare for Final Exam 1 3
1 2
1 2
9 3
1 3
1 2
1 3
9 1
Dönem İçi Notu (DİN) 3 6
Dönem Sonu Sınavı (DSS) 1 3
Total Workload
Total Workload / 30 (s)
ECTS Credit of the Course
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Course Information
  • Course Information
  • Weekly Topics (Content)
  • Sources Used in This Course
  • ECTS credits and course workload