Course Information


Course Information
Course Title Code Semester L+U Hour Credits ECTS
ANALYTICAL CHEMISTRY LABORATUARY II CHM0258 4. Semester 0 + 6 3.0 4.0

Prerequisites None

Language of Instruction English
Course Level Bachelor's Degree
Course Type Compulsory
Mode of delivery
Course Coordinator
Instructors
Assistants
Goals To teach the basic concepts of gravimetric and titrimetric analysis and experimental techniques
Course Content Gravimetric barium analysis, gravimetric analysis of binary mixtures, titrimetric analysis for neutralization, precipitation, complexometric and redox reactions, real sample analysis
Learning Outcomes 1) Apply quantitative analysis techniques
2) 2. During working in the laboratory receives the necessary safety precautions and warnings
3) 3. Recognise tools and utensils used for quantitative analysis allows laboratory
4) 4. Applies the techniques of gravimetric analysis
5) Determines the acidic and basic substances quantitatively
6) Determines the oxidative and reductive substances quantitatively.
7) 7. Determines the complex making substances quantitatively.
8) Chooses an indicator for precipitation, acid-base, complex formation and oxidation-reduction titrations
9) Prepare the sample for analysis, and designs a variety of experiment for quantitative analysis of samples of components.

Weekly Topics (Content)
Week Topics Teaching and Learning Methods and Techniques Study Materials
1. Week Records and material procurement, settlement and cleaning, presentation of equipment and materials Lecture; Question Answer

Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
2. Week Marking of the crucibles, brought to constant weight in the analysis Gravimetric barium analysis Lecture; Question Answer

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
3. Week Continue to gravimetric barium analysis, Filtration of BaSO4 precipitate and brought to constant weighing in the burner Lecture; Question Answer; Problem Solving; Case Study

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
4. Week Gravimetric separation and determination of the two cation mixtures Lecture; Question Answer; Problem Solving; Case Study

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
5. Week Continue to analysis Lecture; Question Answer; Discussion; Case Study

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
6. Week Continue to analysis Lecture; Question Answer; Discussion

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
7. Week Preparation and adjustment of 0.1 M HCl solution and sample analysis with adjusted solutions Lecture; Question Answer; Problem Solving; Discussion

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
8. Week Preparation and adjustment of 0.1 M NaOH solution, determination of acetic acid in vinegar Lecture; Question Answer; Problem Solving; Discussion

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
9. Week Preparation of the 0.05 M AgNO3 solution, adjustment of silver nitrate solution and determination of the chloride by Mohr, fajans and volhard methods Lecture; Question Answer; Problem Solving; Discussion

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
10. Week Preparation and adjustment of Sodium thiosulfate solution and the titrimetric determination of copper,, preparation of 0.02 M KMnO4 solution Lecture; Question Answer; Problem Solving; Discussion

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
11. Week The determination of dissolved oxygen in water, Filtration and adjustment of 0.02 M KMnO4 solution Lecture; Question Answer; Problem Solving; Discussion

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
12. Week Determination of Fe3 + with KMnO4 Lecture; Question Answer; Problem Solving; Discussion

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
13. Week Preparation and adjustment of the K2Cr2O7 solution, chemical oxygen demand (COD) determination in water Lecture; Question Answer; Problem Solving; Case Study

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
14. Week Compensation Lecture; Question Answer

Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)

Sources Used in This Course
Recommended Sources
Analytical Chemistry and Quantitative Analysis, D.Hage, J.D.Carr, Prentice Hall, 2011
Fundamentals of Analytical Chemistry 8th Edition; Skoog, West, Holler, Crouch Translation Editors: E. Kılıç and H. Yılmaz, Bilim Publications, 2004.
Fundamentals of Analytical Chemistry 9th Edition; F. James Holler, Stanley R. Crouch, 2013.

Relations with Education Attainment Program Course Competencies
Program RequirementsContribution LevelDK1DK2DK3DK4DK5DK6DK7DK8DK9
PY15000000000
PY25000000000
PY35000000000
PY45000000000
PY55000000000

*DK = Course's Contrubution.
0 1 2 3 4 5
Level of contribution None Very Low Low Fair High Very High
.

ECTS credits and course workload
Event Quantity Duration (Hour) Total Workload (Hour)
Course Duration (Total weeks*Hours per week) 14 6
Work Hour outside Classroom (Preparation, strengthening) 10 2
Homework 1 5
Midterm Exam 2 5
Time to prepare for Midterm Exam 1 3
Final Exam 1 2
Time to prepare for Final Exam 1 5
Total Workload
Total Workload / 30 (s)
ECTS Credit of the Course
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