Course Information


Course Information
Course Title Code Semester L+U Hour Credits ECTS
INORGANIC CHEMISTRY LABORATORY CHM0422 8. Semester 0 + 6 3.0 5.0

Prerequisites None

Language of Instruction English
Course Level Bachelor's Degree
Course Type Compulsory
Mode of delivery
Course Coordinator
Instructors
Assistants
Goals To provide the connection between the theoretical knowledge of inorganic chemistry and experimental studies and results.
Course Content Laboratory safety, Cytokiometry, Synthesis of alums, Preparation of metal oxides, halides and acetates, Preparation of coordination compounds, Preparation of isomeric complexes, Preparation of dithiyolade and Schiff base complexes, Synthesis of inorganic polymers.
Learning Outcomes 1) He/She uses tools and equipments safely which is used in the inorganic chemistry laboratory for the purpose.
2) He/She describes methods for the preparation of inorganic salts and complexes, associates spectral and structural properties of these compounds with other data.
3) He/She classifies inorganic compounds based on their physical and chemical properties, proposes a method for the synthesis of new coordination compounds.
4) He/She balances and comments to inorganic reactions.
5) He/She selects a suitable method to elucidate the structures of coordination compounds.
6) He/She evaluates and interprets the results obtained from experiments in a group.
7) He/She takes necessary safety precautions for herself/himself and her/his environment in chemistry laboratory studies.

Weekly Topics (Content)
Week Topics Teaching and Learning Methods and Techniques Study Materials
1. Week Introduction: Laboratory safety, preliminary preparations. Lecture; Question Answer; Demonstration
Colloquium; Large Group Discussion
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
2. Week Double Salts: Preparation and applications of alums (Experiment no: 1). Lecture; Question Answer; Demonstration
Colloquium; Large Group Discussion
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
3. Week Cytochiometry: Preparation of lead iodide (PbI2) (Experiment no: 2). Lecture; Demonstration
Colloquium; Large Group Discussion
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
4. Week Acetates: Synthesis of Hg(CH3COO)2 (Experiment no: 3).and Mn(CH3COO)3.2H2O (Experiment no: 4) compounds. Lecture; Question Answer
Colloquium
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
5. Week Salts: Synthesis of (NH4)2SO4CuSO4.nH2O (Experiment no: 5) and (NH4)2SO4NiSO4.6H2O (Experiment no: 6) compounds. Lecture; Question Answer
Colloquium
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
6. Week Metal ammine complexes: Synthesis of [Cu(NH3)4]SO4.H2O (Experiment no: 7) and [Ni(NH3)6Cl2 (Experiment no: 8) complexes. Lecture; Question Answer; Demonstration
Colloquium
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
7. Week Metal acetylacetonate complexes and thin-layer chromatography: Synthesis of [Mn(C5H7O2)3], [Fe(C5H7O2)3], [Cr(C5H7O2)3], [Cu(C5H7O2)2], [Ni(C5H7O2)2] and [Al(C5H7O2)3] complexes and application of thin-layer chromatography for the complexes (Experiment no: 9). Lecture; Question Answer; Demonstration
Colloquium; Large Group Discussion
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
8. Week Metal dioxalate complexes and preparation of isomeric complexes: Syntheses of trans- K[Cr(C2O4)2(H2O)2].3H2O complex and separation of cis- and trans-isomers from each other (Experiment no: 10). Lecture; Question Answer
Debate
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
9. Week Metal trioxalate complexes: Synthesis of K3[Cr(C2O4)3].3H2O (Experiment no: 11) and K3[Al(C2O4)3].3H2O (Experiment no: 12) complexes. Lecture; Question Answer; Demonstration
Colloquium; Large Group Discussion
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
10. Week Preparation of Schiff base complexes with some metal cations: Synthesis of various Schiff base complexes including nickel (II) and copper (II) ions (Experiment no: 13). Lecture; Question Answer; Demonstration
Colloquium
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
11. Week Cobalt ammine complexes: Synthesis of [Co(NH3)4CO3]NO3 (Experiment no: 14) and [Co(NH3)5Cl]Cl2 (Experiment no: 15) complexes. Lecture; Question Answer; Demonstration
Colloquium; Large Group Discussion
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
12. Week Synthesis of other complexes: Synthesis of K3[Cr(O2)4] (Experiment no: 16) and [(CH3CH2)2NH2]2CuCl4 (Experiment no: 17) complexes. Lecture; Question Answer; Demonstration
Colloquium
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
13. Week Conducting experiments that cannot be done on time: All experiments. Lecture; Question Answer; Demonstration
Colloquium
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)
14. Week Inorganic Polymers: Obtaining polymer paper. Lecture; Question Answer; Case Study
Colloquium
Problem Based Learning
Report (Including Preparation and presentation Time) Practice (Teaching Practice, Music/Musical Instrument Practice, Statistics, Laboratory, Field Work, Clinic and Polyclinic Practice)

Sources Used in This Course
Recommended Sources
Inorganic Experiments; J. D. Woollins, Wiley-VCH, 2002.

Relations with Education Attainment Program Course Competencies
Program RequirementsContribution LevelDK1DK2DK3DK4DK5DK6DK7
PY155555555
PY255555555
PY355555555
PY455555555
PY555555555

*DK = Course's Contrubution.
0 1 2 3 4 5
Level of contribution None Very Low Low Fair High Very High
.

ECTS credits and course workload
Event Quantity Duration (Hour) Total Workload (Hour)
Course Duration (Total weeks*Hours per week) 14 6
Work Hour outside Classroom (Preparation, strengthening) 14 2
Report (Including Preparation and presentation Time) 14 1
Midterm Exam 1 2
Time to prepare for Midterm Exam 1 12
Final Exam 1 2
Time to prepare for Final Exam 1 12
Total Workload
Total Workload / 30 (s)
ECTS Credit of the Course
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